If you go here http://www.ti.com/product/MSP430FR2433/toolssoftware there are is MSP430FR243x, MSP430FR253x, MSP430FR263x Code Examples (Rev. C) ZIP file (slac700c.zip). In this archive are Assembly_CCS and Assembly_IAR directories with examples codded in assembler. Detailed description of peripherals can be found in family datasheet (slau445) MSP430FR4xx and MSP430FR2xx Family User's Guide (Rev. H).
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